87.060.30 (Solvents) 标准查询与下载



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1.1 This test method covers the determination of the miscibility of water-soluble solvents with water. While written specifically for testing acetone, isopropyl alcohol (isopropanol), and methyl alcohol (methanol), the method is suitable for testing most water-soluble solvents. 1.2 This test method serves to detect water-immiscible contaminants qualitatively; the level of detection of these impurities varies widely with both the type of solvent and the type of impurity. 1.3 The level of detection of water-insoluble materials depends upon the solvent tested and the type of impurity or impurities present, that is paraffin, olefin, aromatic, high molecular weight alcohol, or ketone, etc. There is, therefore, no specific level of impurity detected by this procedure. Note-This test method is normally performed at ambient, but other temperatures may be used as specified by the consumer and supplier. 1.4 This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.> 1.5 For specific hazard information and guidance, consult the supplier''s Material Safety Data Sheet for materials listed in this test method.

Standard Test Method for Water Miscibility of Water-Soluble Solvents

ICS
87.060.30 (Solvents)
CCS
G60
发布
1998
实施

Many naval stores products contain water as a result of the processes used for their production. Typically refined products such as terpenes, pine oil, tall oil fatty acids, and distilled tall oil contain only traces of water, but crude tall oil might contain 0.5 to 2.5 % of water. Although the Karl Fischer and coulometric methods are most applicable to low levels of moisture, these can be and are used at higher levels. The azeotropic distillation method is generally used at higher levels.1.1 These test methods cover the quantitative determination of dissolved or occluded water present in any proportion in liquid naval stores, such as turpentine, pinene, dipentene, pine oil, tall oil, and tall oil fatty acids. Three methods of moisture testing are included. The Karl Fisher titration method is the preferred method for testing tall oil, Test Methods D 803. 1.1.1 The Karl Fischer Titration method is based on the reaction between water and a complex reagent consisting of iodine, sulfur dioxide, pyridine, and methanol, whereby the iodine is converted to a colorless compound. The appearance of a persistent iodine color in the reaction mixture indicates the complete removal of free water by reaction with the reagent, and the endpoint may be measured colorimetrically. Automatic titrators find this endpoint by the restoration of a current strength when the resistance provided by the presence of water is eliminated. Amperometric automatic titrators find this endpoint by detecting the current flow that occurs once water is eliminated. 1.1.2 The coulometric titration method determines water content by electronic integration of a current sufficient to generate the precise amount of iodine from the required reagent to react with the water in the sample. 1.1.3 The azeotropic method utilizes the relatively low boiling point of water, as compared with other sample constituents, in a toluene or xylene matrix so that water is collected in a trap and measured. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Water in Liquid Naval Stores

ICS
87.060.30 (Solvents)
CCS
G50
发布
1998
实施

1.1 This specification covers benzene-545. 1.2 The following applies to all specified limits in this standard: for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off "to the nearest unit" in the last right-hand digit used in expressing the specification limit in accordance with the rounding-off method in Practice E 29. 1.3 Consult current OSHA regulations and supplier's Material Safety Data Sheets for all materials used in this specification.

Standard Specification for Refined Benzene-545

ICS
87.060.30 (Solvents)
CCS
G16
发布
1998
实施

1.1 This specification covers the following kinds of spirits of turpentine as defined by the Naval Stores Act and Terminology D 804: gum spirits of turpentine, steam-distilled wood turpentine, sulfate wood turpentine, and destructively-distilled wood turpentine. 1.2 The purchaser should specify the kind of spirits of turpentine desired. 1.3 This specification is no longer widely used as it only specifies physical characteristics and not chemical composition. This specification was developed when the chief use for turpentine was as a solvent. Currently, especially in the United States, only a very limited quantity of turpentine is used as a solvent. Its main end use is as a raw material for the preparation of polyterpene type resins and synthetic organic chemicals. In spite of its limited application as a solvent, and hence the limited use of this specification, it is considered to be important to retain this specification. When information is required on chemical composition, gas chromatography is the recommended procedure (see Test Method D3009 ).

Standard Specification for Spirits of Turpentine

ICS
87.060.30 (Solvents)
CCS
B72
发布
1997
实施

1.1 This test method covers the visual measurement of the color of halogenated organic solvents and their admixtures. It is valid for values of 50 platinum-cobalt (Pt-Co) units or less. 1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. >

Standard Test Method for Color of Halogenated Organic Solvents and Their Admixtures (Platinum-Cobalt Scale)

ICS
87.060.30 (Solvents)
CCS
发布
1997
实施

1.1 This specification covers diacetone alcohol. 1.2 For specific hazard information and guidance, consult the supplier's Material Safety Data Sheet.

Standard Specification for Diacetone Alcohol

ICS
87.060.30 (Solvents)
CCS
G17
发布
1997
实施

1.1 These test methods cover procedures for sampling and testing turpentine, as defined by the Naval Stores Act and Terminology D804. These test methods are also used for the sampling and testing of pinenes, the major components of most turpentines. 1.2 These test methods primarily measure the physical rather than the chemical properties of turpentines and pinenes. As turpentines and pinenes are currently used chiefly as chemical raw materials for the production of resins and synthetic organic chemicals, chemical composition is also very important. Consequently, testing the chemical composition of turpentines and pinenes by gas chromatography has displaced these test methods to a large extent. (See for example Test Method D3009.) 1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.>

Standard Test Methods of Sampling and Testing Turpentine

ICS
87.060.30 (Solvents)
CCS
G50
发布
1997
实施

1.1 These test methods cover the determination of ethylbenzene and total eight-carbon (C8) and heavier aromatics in the concentration range from 0.1 to 30 % in mineral spirits having a distillation range from 149 to 210oC (300 to 410oF) as determined by Test Method D86. The procedures permit the identification and calculation of concentrations of aromatic components to 0.1 volume %.1.2 It is recognized by analytical chemists that a single column gas chromatography analysis of an unknown sample is risky. In such cases, multiple and different analytical techniques must be used for absolutely positive identification, for example, several different gas chromatography columns, gas chromatography/mass spectrometer, or gas chromatography/infrared, etc. In these test methods the material is known and is clearly defined.1.3 Oxygenated compounds, if present, may interfere and cause erroneous results. Such oxygenated compounds are not normally present in mineral spirits.1.4 Three test methods are covered as follows:1.4.1 Test Method A, measurement of ethylbenzene content, C8 plus higher aromatics (except ethylbenzene), and total aromatics by means of a single packed column gas chromatographic analysis.1.4.2 Test Method B, measurement of ethylbenzene content by means of a rapid packed column gas chromatographic analysis.1.4.3 Test Method C, measurement of ethylbenzene content, C8 plus higher aromatics (except ethylbenzene) and total aromatics by means of a capillary column gas chromatographic analysis.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.1.6 For hazard information and guidance, see the supplier's Material Safety Data Sheet.

Standard Test Methods for Aromatics in Mineral Spirits by Gas Chromatography

ICS
87.060.30 (Solvents)
CCS
E33
发布
1997
实施

1.1 These test methods cover procedures for sampling and testing dipentene and related terpene solvents, consisting chiefly of monocyclic terpene hydrocarbons distilling above the range for turpentine. 1.2 The procedures given in these test methods appear in the following order: Section Sampling 4 Detection and Removal of Separated Water 5 Appearance 6 Color 7 Odor 8 Specific Gravity 9 Refractive Index 10 Distillation 11 Flash Point 12 Dissolved Water 13 Aniline Point and Mixed Aniline Point 14 1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.>

Standard Test Methods for Sampling and Testing Dipentene

ICS
87.060.30 (Solvents)
CCS
G17
发布
1997
实施

1.1 This test method covers the evaluation of the corrosiveness to metals by halogenated organic solvents and their admixtures for cold cleaning applications. Note 1-The test method described herein is an adaptation of Test Method D130. 1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Metal Corrosion by Halogenated Organic Solvents and Their Admixtures

ICS
87.060.30 (Solvents)
CCS
发布
1996
实施

1.1 This specification covers four types of moderately volatile hydrocarbon solvents, mainly aliphatic in composition and normally petroleum distillates. These solvents are used primarily by the coatings industry and are commonly referred to as VMP naphthas. 1.2 For specific hazard information and guidance, see the supplier's Material Safety Data Sheet for materials listed in this specification.

Standard Specification for VMP Naphthas

ICS
87.060.30 (Solvents)
CCS
G17
发布
1996
实施

1.1 This specification covers two types of aromatic hydrocarbon solvents, normally petroleum distillates, having high flash points, moderately low volatility, and a distillation range of approximately 50oF (30oC). These solvents are used primarily by the coatings industry and are commonly referred to as high-flash aromatic naphthas. 1.2 For specific hazard information and guidance, see the supplier's Material Safety Data Sheet for materials listed in this specification.

Standard Specification for High-Flash Aromatic Naphthas

ICS
87.060.30 (Solvents)
CCS
G52
发布
1996
实施

1.1 This test method covers the determination of the nonvolatile matter in volatile solvents for use in paint, varnish, lacquer, and related products. 1.2 This standard does not purport to address all of the safety concerns,, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 5. 1.3 For hazard information and guidance, see the supplier''s Material Safety Data Sheet for materials listed in this test method.

Standard Test Method for Nonvolatile Matter in Volatile Solvents for Use in Paint, Varnish, Lacquer, and Related Products

ICS
87.060.30 (Solvents)
CCS
发布
1996
实施

1.1 This test method describes a procedure for determining the sustained burning characteristics of mixtures of flammable and nonflammable liquids and also mixtures containing liquids with widely different flash points. 1.2 This standard should be used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions and should not be used to describe or appraise the fire-hazard or fire-risk of materials, products, or assemblies under actual fire conditions. However, results of the test may be used as elements of a fire-hazard assessment or a fire-risk assessment which takes into account all of the factors which are pertinent to an assessment of the fire hazard or fire risk of a particular end use. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Sustained Burning of Liquid Mixtures Using the Small Scale Open-Cup Apparatus

ICS
87.060.30 (Solvents)
CCS
E30
发布
1996
实施

1.1 This test method covers the determination of the volume ratio of hydrocarbon diluent to active solvent required to cause persistent heterogeneity (precipitation) in a solution of cellulose nitrate. 1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 6. 1.3 For hazard information and guidance, see the supplier''s Material Safety Data Sheet.

Standard Test Method for Dilution Ratio of Active Solvents in Cellulose Nitrate Solutions

ICS
87.060.30 (Solvents)
CCS
发布
1996
实施

1.1 This test method covers the determination of the total acid acceptance including amine and neutral type (alpha epoxide) stabilizers in halogenated organic solvents. 1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 7.

Standard Test Method for Total Acid Acceptance of Halogenated Organic Solvents (Nonreflux Methods)

ICS
87.060.30 (Solvents)
CCS
发布
1996
实施

1.1 This test method covers the determination of total acidity as acetic acid, in concentrations below 0.05%, in organic compounds and hydrocarbon mixtures used in paint, varnish, and lacquer solvents and diluents. It is known to be applicable to such mixtures as low molecular weight saturated and unsaturated alcohols, ketones, ethers, esters, hydrocarbon diluents, naphtha, and other light distillate petroleum fractions. 1.2 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of whoever uses this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 1.3 For specific hazard information and guidance consult supplier''s Material Safety Data Sheet.

Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products

ICS
87.060.30 (Solvents)
CCS
发布
1996
实施

1.1 This guide covers procedures for the sampling and testing of volatile solvents used in the manufacture of paint, lacquer, varnish, and related products. The test methods are listed in Table 1.1.2 For specific hazard information and guidance, see Suppliers' Material Safety Data Sheet for materials listed in this guide.1.3 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Guide for Sampling and Testing Volatile Solvents and Chemical Intermediates for Use in Paint and Related Coatings and Material

ICS
87.060.30 (Solvents)
CCS
G60;G50
发布
1996
实施

1.1 This is a screening test method to determine if sufficient inhibitors are present in 1,1,1-trichloroethane to provide at least minimal stability in the presence of aluminum. 1.2 Solvent passing this test may not be stable for all applications. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. A specific hazard statement is given in Section 6.

Standard Test Method for Aluminum Scratch of 1,1,1-Trichloroethane to Determine Stability

ICS
87.060.30 (Solvents)
CCS
发布
1996
实施

These tests are to be used as a guide in selecting or eliminating certain solvents or grades of solvents used for cleaning or degreasing metal parts.1.1 This test method covers the evaluation of the corrosiveness to metals by halogenated organic solvents and their admixtures for cold cleaning applications. Note 1The test method described herein is an adaptation of Test Method D 130.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Metal Corrosion by Halogenated Organic Solvents and Their Admixtures

ICS
87.060.30 (Solvents)
CCS
H25
发布
1996
实施



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